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. 1998 Feb 27;61(2):297-8.
doi: 10.1021/np970394g.

The Synthesis of Phycopsisenone, a New Phenolic Secondary Metabolite from the Sponge Phycopsis sp

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The Synthesis of Phycopsisenone, a New Phenolic Secondary Metabolite from the Sponge Phycopsis sp

GL Kad et al. J Nat Prod. .

Abstract

A short first total synthesis of phycopsisenone (1) utilizing microwave irradiation-induced aldol condensation and TiCl4-catalyzed reaction of silyl enol ether (3) with acetone as key steps has been achieved in 29.4% overall yield.

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