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Lisinopril dihydrate: single-crystal x-ray structure and physicochemical characterization of derived solid forms.
Sorrenti M, Catenacci L, Cruickshank DL, Caira MR. Sorrenti M, et al. J Pharm Sci. 2013 Oct;102(10):3596-603. doi: 10.1002/jps.23660. Epub 2013 Jul 19. J Pharm Sci. 2013. PMID: 23873413
Screening for new solid forms of the antihypertensive lisinopril was performed by recrystallization of the commercial form, lisinopril dihydrate, from various solvents and by exposing the product of its dehydration to a series of vapors under controlled conditions. …
Screening for new solid forms of the antihypertensive lisinopril was performed by recrystallization of the commercial form, lisino …
Thermal-Dependent dehydration process and intramolecular cyclization of lisinopril dihydrate in the solid state.
Wang SL, Lin SY, Chen TF. Wang SL, et al. Chem Pharm Bull (Tokyo). 2000 Dec;48(12):1890-3. doi: 10.1248/cpb.48.1890. Chem Pharm Bull (Tokyo). 2000. PMID: 11145138
The results indicate that the dehydration from the solid-state lisinopril dihydrate had a two-step process from dihydrate to monohydrate at 76 degrees C and then from monohydrate to anhydrate at 99-101 approximately C, which could be clearly observed from the above …
The results indicate that the dehydration from the solid-state lisinopril dihydrate had a two-step process from dihydrate to monohydr …
Multivariate chemometric approach to thermal solid-state FT-IR monitoring of pharmaceutical drug compound.
Tan WJ, Widjaja E. Tan WJ, et al. J Pharm Sci. 2008 Aug;97(8):3379-87. doi: 10.1002/jps.21275. J Pharm Sci. 2008. PMID: 18085713
The resulting pure component spectral estimates were then further refined using alternating least squares (ALS). In current study, four pure component spectra, that is, lisinopril dihydrate, monohydrate, anhydrate, and diketopiperazine (DKP) were all resolved and th …
The resulting pure component spectral estimates were then further refined using alternating least squares (ALS). In current study, four pure …