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Alkylation of a dimolybdenum SO bridge, subsequent reactions, and characterization of the thioperoxide bridge.
Tuong CM, Hammons WK, Howarth AL, Lutz KE, Maduvu AD, Haysley LB, Allred BR, Hoyt LK, Mashuta MS, Noble ME. Tuong CM, et al. Inorg Chem. 2009 Jun 1;48(11):5027-38. doi: 10.1021/ic9002093. Inorg Chem. 2009. PMID: 19466806
The SO bridge of the complex, [Mo(2)(NTo)(2)(S(2)P(OEt)(2))(2)(mu-O(2)CMe)(mu-SBn)(mu-SO)], 1, displayed nucleophilicity at O, giving alkylation products [Mo(2)(NTo)(2)(S(2)P(OEt)(2))(2)(mu-O(2)CMe)(mu-SBn)(mu-SOR)](+), 4(+), which contained the thioperoxide …
The SO bridge of the complex, [Mo(2)(NTo)(2)(S(2)P(OEt)(2))(2)(mu-O(2)CMe)(mu-SBn)(mu-SO)], 1, displayed nucleophilicity at O, …
Ligand substitution behavior of Ru(6)(mu(6)-C)(CO)(17) with unsaturated diphosphines: facile capping of a polyhedral face and photochemically promoted P-C bond cleavage in the cluster Ru(6)(mu(6)-C)(CO)(14)(mu(3)-bpcd).
Kandala S, Hammons C, Watson WH, Wang X, Richmond MG. Kandala S, et al. Dalton Trans. 2010 Feb 14;39(6):1620-9. doi: 10.1039/b915337c. Epub 2009 Dec 14. Dalton Trans. 2010. PMID: 20104326
Near-UV irradiation of leads to P-C bond cleavage and the formation of phosphido-bridged cluster Ru(6)(mu(6)-C)(CO)(13)[mu(3)-C[double bond, length as m-dash]C(PPh(2))C(O)CH(2)C(O)](mu-PPh(2)) () in essentially quantitative yield. The reaction between and the ligand …
Near-UV irradiation of leads to P-C bond cleavage and the formation of phosphido-bridged cluster Ru(6)(mu(6)-C)(CO)(13)[mu(3)-C[double bond, …