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23752753,16242883,25336421,21083152,23969330,23721687,23788325,28231528,26269925,26437511,24081463,18180126,12867148,28279928,28256254,17994660,22265473,34227756,24209357,18778828,29414013,25336417,29762685,16912986,25978495,25336416,22162441,22351183,16329084,26429108,16280226,20486265,14616013,25260345,29059617,22658656,27070830,11092605,25476333,25751287,19757407,30280447,29054149,28776774,18798699,24267061,24853620,17405144,16049948,23453678,28238322,21936562,23706957,10070765,20685449,26879646,11002275,26183111,22290710,31226425,28875855,21481400,22575670,32796601,30500460,29579733,16158985,24769301,28024262,25296128,25797717,17377776,28248501,28512176,32366050,12362389,26797969,26643725,27769407,20942391,22178334,16870197,17624026,29943976,22247862,29214535,18578518,22337798,30030347,33010603,22265352,30466025,13680063,19635380,12504330,28027837,26395784,11704957,21756165,30658005,30921495,9008869,22888997,28265711,20926086,24148498,7096521,23220754,24084658,28926062,19806741,24657819,31438569,11403494,14971488,32387747,28992990,27825701,31463842,11055717,28531831,29974421,32814262,31676090,16008047,12877183,28619585,34324943,30513899,29903190,24800968,12705965,10430788,29229330,3597621,30106288,24084660,10226876,11080866,33280701,32814259,29373129,33280999,24685167,29343620,12350089,30599277,11805734,24265307,25644491,27426455,31209164,16787159,24084659,32371324,28330782,32113121,32691615,25840658,15088751,30024655,27667648,31315205,32045999,10096833,14623588,10784161,24358770,21444173,32360549,1564106,30651335,12033491,31252628,16864507,27426453,28620306,31250064,10704011,32113524,31971527,11377016,32681152,29517997,34811999,26585206,7599744,27363664,28825428,24309715,30232139,11092602,25257980,11045496,31071579,33740606,30793214,31843988,32333306,21520717,33990421,26830636,33628763,28890270,30502186,1747398,32408991,11929670,24894111,18334084,11554415,29330878,10774537,29370527,15844518,17877437,34212585,28882340,33965022,27702614,33923004,8972626,11694312,25464997,14763799,31450417,32348952,30693720,32128644,14763756,12580495,30663714,9234855,24125719,20526353,31369833,23106399,33458791,11320422,9278896,30111228,12049976,29505232,28739275,32970370,18827388,24929909,34153734,8984892,34212580,25236197,11092604,23442929,9300914,28490051,33822260,25537130,34782443,19508399,31113532,31216665,15777210,14661927,30925345,10910213,12408905,24595746,28211639,30892803,31202351,30444314,28778531,32706176,30653352,10782386,18084916,29897176,9083829,28928293,31352172,15974132,30668111,32887036,31101707,17154121,10405597,31613088,32029113,14656591,7807124,14971492,29764677,30848316,9919951,28380387,26331594,24392628,30255625,31505485,14570215,30661760,33855234,31469924,30659562,7735475,11272313,1298391,11377035,19084633,21723140,19601826,15295885,21731458,11192153,34213179,11835254,29958681,31970954,30471289,31347114,11043587,20447930,28942996,17051523,33479819,31943846,34543882,20140083,19772737,19028813,33189291,27475993,12458932,28764013,7127804,31067700,10572974,11805733,30238638,29654588,19086313,30876579,29491650,10933550,31128881,30902276,10895949,24757942,26795737,30079731,29437387,29784410,21525822,27712885,31255758,9079206,32505112,15926671,30335379,8887722,30027362,27584954,10572973,22292474,34666267,34097785,21396233,19714883,31698885,33057737,17390611,33744596,7913965,33426324,1873304,33908004,11817044,9656157,34380070,15595533,11824396,14565558,10594907,34590821,20873583,25294001,28538204,30381003,29886002,31027298,14509431,29097223,33255692,32112476,11092603,8887713,32633064,29623538,32372465,28301728,30609525,31420503,33142699,8913839,32272592,30289623,30779381,27325598,29887729,16114257,30158239,16634283,18968548,10669295,34071244,16224955,33199517,31829054,10704117,33721827,30810397,12173177,27644982,31515074,33593699,29403837,30502919,31372702,30501039,34710726,30952244,25368916,18520144,31820027,2026705,30830245,11093654,15759752,33892395,17500369,12877178,30597685,33913944,31250495,31207650,31498582,10526788,26275862,31847163,21888316,23232239,32918172,34089713,26964227,16224969,33660499,12667931,25340205,34000097,9165202,11572402,23307153,28629236,32718778,33648641,32794693,21811394,29475628,12350088,29381342,33379100,23451509,32307348,18276099,17614233,2374404,2026711,10985544,33804650,11510839,23561912,30292304,30378212,22290485,12609666,31302170,16224967,11153941,11092606,31374921,3597616,14738913,26635443,31785932,34660534,26394146,11209904,27274730,11762773,23574679,12726840,32744053,8581121,32899296,28700970,27215462,10703982,34482900,14971487,34469750,26372444,32250027,28340472,31883609,31033229,30983324,25005992,10637049,30005987,16749531,11355815,34110145,26929579,15825641,32850646,33233095,10950296,31250320,10941673,11924985,34761922,30905375,32247161,34826946,32232571,7306684,30720234,29403898,10885057,25690297,11217765,10727136,33834449,33037749,33265036,33197986,28791049,33610133,27018189,11472225,34724607,15497700,30960448,31243828,27029304,34213154,8429076,28208280,31489561,1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Page 1

Automated Solid Phase Extraction (SPE) LC/NMR Applied to the Structural Analysis of Extractable Compounds from a Pharmaceutical Packaging Material of Construction.

Norwood DL, Mullis JO, Davis M, Pennino S, Egert T, Gonnella NC. Norwood DL, et al. PDA J Pharm Sci Technol. 2013 May-Jun;67(3):267-87. doi: 10.5731/pdajpst.2013.00920. PDA J Pharm Sci Technol. 2013. PMID: 23752753

The use of LC/MS, GC/MS, and LC/NMR hyphenated techniques to identify a drug degradation product in pharmaceutical development.

Pan C, Liu F, Ji Q, Wang W, Drinkwater D, Vivilecchia R. Pan C, et al. J Pharm Biomed Anal. 2006 Feb 24;40(3):581-90. doi: 10.1016/j.jpba.2005.08.020. Epub 2005 Oct 20. J Pharm Biomed Anal. 2006. PMID: 16242883

A Method Utilizing Ultra-High Performance Liquid Chromatography with Ultraviolet and Mass Spectrometric Detection for the Analysis of Material Extracts Produced during a Controlled Extraction Study.

Zdravkovic SA, Bruss MD, Piccoli RF, Wood DM. Zdravkovic SA, et al. PDA J Pharm Sci Technol. 2014 Sep-Oct;68(5):504-26. doi: 10.5731/pdajpst.2014.00992. PDA J Pharm Sci Technol. 2014. PMID: 25336421

LC-SPE-NMR-MS: a total analysis system for bioanalysis.

Schlotterbeck G, Ceccarelli SM. Schlotterbeck G, et al. Bioanalysis. 2009 Jun;1(3):549-59. doi: 10.4155/bio.09.50. Bioanalysis. 2009. PMID: 21083152 Review.

Forced degradation and impurity profiling: recent trends in analytical perspectives.

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