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29343617,33990422,29030531,32679217,22492599,25336420,26852839,27178628,26316044,37244516,21319164,36933655,32871152,36404459,25740412,33585996,33890418,19634353,33452050,32565353,32817321,39164114,24643773,21502072,37536577,24643749,25691719,22293836,25256796,32771345,26423033,24729310,29853611,27328279,21538214,30642195,32127655,26190624,37714568,27620008,28089934,24265307,27233685,35365551,23280943,8846058,30391415,32534032,27773525,39079589,12614410,33633285,26889055,9615155,24382812,28819049,39179394,30788149,37142129,11244337,34717776,34400526,26048747,21780119,23023774,32739384,35857984,28639328,30914272,26413998,29421215,37302655,15975470,28367509,37188533,18695632,31628922,34623967,22293523,30471289,27639706,28632533,34024140,28841584,11057095,30790580,38220088,28207606,33029664,30910872,34131016,37451836,22794526,26474763,26797967,17295521,35122830,25800359,30562565,26659102,31369770,32956210,31689431,33069712,16337954,39179391,38983507,37382286,18759384,38556370,23625851,33217252,16205578,38705829,15656089,27020987,22429889,35715871,19894257,19461812,23595940,1995035,28603019,30168715,24668602,28465152,34310973,30153890,27516487,21319034,22511025,20527517,38183130,28216023,26296188,29256738,37085185,30296419,32673625,7704926,37580129,19865461,18324116,38378097,37936232,36122618,36572486,30196040,19483420,38113997,33983076,25364017,39137820,35598767,36716845,32311476,25228786,31669608,26797970,34551352,38277478,36626504,36531591,34713903,30801979,38014840,33122049,31780932,37335669,34843652,22368463,31696930,33272095,19183611,2975573,38580881,29626532,30720284,31136765,34632573,39307455,34237379,16149343,35779650,23129865,3542458,19529611,20953747,31043001,1769068,34024924,8018315,17119559,31432896,30422015,3322733,38326531,33504510,37665244,30651339,32752547,7379802,30828350,32107671,37989952,19340102,24098867,38175634,33307040,33435177,38175624,37268032,10474890,21948455,32415524,32414526,23486006,32001031,34064513,35201213,36815817,22767879,9152087,21667187,35854079,19828931,30385286,30934705,35948157,30839956,32256047,35144740,33189808,37112653,10928904,32244706,2278394,36137451,38178468,35882533,34160142,7553439,31370503,38949471,31420501,22293837,1457923,32933199,31873446,32412022,36785346,37941961,35893510,5651051,29408118,19881853,32225244,37303768,12482012,10469100,35839866,22802102,20076777,26555667,30866475,33875826,525300,3559960,17167559,33918507,18593458,25182472,37157332,34619153,7714893,39146122,30839519,37648725,31370474,23071944,22031733,33023210,36002916,14960067,11931796,35218897,12197656,18264221,37249498,32990191,32403543,39302177,19277082,31013859,38631943,30315809,35471302,13061297,31429832,32647349,17994143,32513992,19516765,36242371,37966767,34263784,32752824,18040340,18349968,35629699,33577522,36340539,36347268,18059746,14091934,18516110,30367137,37154670,34958824,33878409,34613267,38138681,15015528,10905312,5139189,8694222,30120334,36194700,16389850,37971165,39140883,38853831,17572731,35683189,37067124,35473124,32227973,27110468,13252104,29116223,19516621,31684586,18264431,37101849,37837137,33379523,4850300,18357298,36821263,36785134,18253269,4184115,20721672,13030671,17932521,32565046,37932965,31730778,18345113,12099592,34119806,30407404,23387635,6850363,10866769,35269130,20245301,16231799,35471306,15404603,37020326,18134847,15434372,15400958,39087415,18140470,14842112,14825065,14842111,36079316,30073643,30073644,31873550,13093892,13264620,13696137,13683245,18101907,13114693,14491899,13985834,14900975,15408340,11936779,15409217,13486499,32507463,13202460,21356931,32225591,6467869,13119016,33255719,25942888,937709,31948372,20257131,12153072,37008104,37096477,36617351,37398627,30770064,14805114,13984400,3399579,13847452,6025217,4725542,38294371,4014401,18100431,18338013,26417170,20267680,23542289,7595692,23542290,34189893,17676132,38081270,35345232,37046006,35772438,31739529,37698317,34851896,18357000,30075656,31062221,15449467,3381474,12916608,36298290,16902643,27512177,37604600,18115766,18026559,17282274,21137933,37132870,18264487,19742022,10236234,33536182,37133151,30938795,32438904,36570625,18131524,12099596,32715070,5339364,31406936,35615656,19829570,19802094,33648074,13009208,37815492,18213102,18204546,472015,10007433,22556891,13330825,19802096,9914003,19981916,9902945,9953278,37910890,10470039,9913216,10529822,22485729,31363532,9906495,18195993,17144355[uid]

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Methods To Determine the Silicone Oil Layer Thickness in Sprayed-On Siliconized Syringes.

Loosli V, Germershaus O, Steinberg H, Dreher S, Grauschopf U, Funke S. Loosli V, et al. PDA J Pharm Sci Technol. 2018 May-Jun;72(3):278-297. doi: 10.5731/pdajpst.2017.007997. Epub 2018 Jan 17. PDA J Pharm Sci Technol. 2018. PMID: 29343617

Method Comparison Study-One Step Forward toward Robust Silicone Layer Thickness Measurements.

Lotfi S, Montagner F, Proff C, Dreher S, Grauschopf U, Zorzi C, Pinato O, Panighello S, Funke S. Lotfi S, et al. PDA J Pharm Sci Technol. 2021 Nov-Dec;75(6):474-489. doi: 10.5731/pdajpst.2020.012567. Epub 2021 May 14. PDA J Pharm Sci Technol. 2021. PMID: 33990422

Impact of Drug Formulation Variables on Silicone Oil Structure and Functionality of Prefilled Syringe System.

Shi GH, Gopalrathnam G, Shinkle SL, Dong X, Hofer JD, Jensen EC, Rajagopalan N. Shi GH, et al. PDA J Pharm Sci Technol. 2018 Jan-Feb;72(1):50-61. doi: 10.5731/pdajpst.2017.008169. Epub 2017 Oct 12. PDA J Pharm Sci Technol. 2018. PMID: 29030531

Method to Determine Syringe Silicone Oil Layer Heterogeneity and Investigation of its Impact on Product Particle Counts.

Cua M, Martin D, Meza P, Torraca G, Pearson T, Cao S, Yang C. Cua M, et al. J Pharm Sci. 2020 Nov;109(11):3292-3299. doi: 10.1016/j.xphs.2020.07.012. Epub 2020 Jul 15. J Pharm Sci. 2020. PMID: 32679217 Free PMC article.

Syringe siliconization process investigation and optimization.

Chan E, Hubbard A, Sane S, Maa YF. Chan E, et al. PDA J Pharm Sci Technol. 2012 Mar-Apr;66(2):136-50. doi: 10.5731/pdajpst.2012.00856. PDA J Pharm Sci Technol. 2012. PMID: 22492599

Characterization of the initial level and migration of silicone oil lubricant in empty prefilled syringes for biologics using infrared spectroscopy.

Bee JS, Frey VV, Javed U, Chung J, Corcoran ML, Roussel PS, Krause SO, Cash PW, Bishop SM, Dimitrova MN. Bee JS, et al. PDA J Pharm Sci Technol. 2014 Sep-Oct;68(5):494-503. doi: 10.5731/pdajpst.2014.00991. PDA J Pharm Sci Technol. 2014. PMID: 25336420

Evaluation of Incremental Siliconization Levels on Soluble Aggregates, Submicron and Subvisible Particles in a Prefilled Syringe Product.

Bai S, Landsman P, Spencer A, DeCollibus D, Vega F, Temel DB, Houde D, Henderson O, Brader ML. Bai S, et al. J Pharm Sci. 2016 Jan;105(1):50-63. doi: 10.1016/j.xphs.2015.10.012. Epub 2015 Dec 22. J Pharm Sci. 2016. PMID: 26852839

Optimization of the bake-on siliconization of cartridges. Part I: Optimization of the spray-on parameters.

Funke S, Matilainen J, Nalenz H, Bechtold-Peters K, Mahler HC, Friess W. Funke S, et al. Eur J Pharm Biopharm. 2016 Jul;104:200-15. doi: 10.1016/j.ejpb.2016.05.007. Epub 2016 May 10. Eur J Pharm Biopharm. 2016. PMID: 27178628

Analysis of thin baked-on silicone layers by FTIR and 3D-Laser Scanning Microscopy.

Funke S, Matilainen J, Nalenz H, Bechtold-Peters K, Mahler HC, Friess W. Funke S, et al. Eur J Pharm Biopharm. 2015 Oct;96:304-13. doi: 10.1016/j.ejpb.2015.08.009. Epub 2015 Aug 24. Eur J Pharm Biopharm. 2015. PMID: 26316044

Variables Impacting Silicone Oil Migration and Biologics in Prefilled Syringes.

Gentile K, Huang C, Liu X, Whitty-Léveillé L, Hamzaoui H, Cristofolli E, Rayfield W, Afanador NL, Mittal S, Krishnamachari Y, Xi H, Zhao X. Gentile K, et al. J Pharm Sci. 2023 Aug;112(8):2203-2211. doi: 10.1016/j.xphs.2023.05.017. Epub 2023 May 25. J Pharm Sci. 2023. PMID: 37244516

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