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trans-Dichlorotetrakis(4-methylpyrimidine-N1)ruthenium(II).
Bellucci C, Cini R. Bellucci C, et al. Acta Crystallogr C. 2001 Sep;57(Pt 9):1039-40. doi: 10.1107/s0108270101009647. Epub 2001 Sep 11. Acta Crystallogr C. 2001. PMID: 11588363
The title compound, trans-[Ru(II)Cl(2)(N(1)-mepym)(4)] (mepym is 4-methylpyrimidine, C(5)H(6)N(2)), obtained from the reaction of trans,cis,cis-[Ru(II)Cl(2)(N(1)-mepym)(2)(SbPh(3))(2)] (Ph is phenyl) with excess mepym in ethanol, has fourfold crystallographic symmet …
The title compound, trans-[Ru(II)Cl(2)(N(1)-mepym)(4)] (mepym is 4-methylpyrimidine, C(5)H(6)N(2)), obtained from the reaction …
Combined experimental-theoretical characterization of chelidamate nickel complex with 4-methylpyrimidine.
Vural H, Uçar I, Soylu MS. Vural H, et al. Spectrochim Acta A Mol Biomol Spectrosc. 2016 Jan 5;152:584-90. doi: 10.1016/j.saa.2014.12.118. Epub 2015 Jan 20. Spectrochim Acta A Mol Biomol Spectrosc. 2016. PMID: 25659755
A new chelidamate complex of nickel(II) ion, [Ni(chel)(H2O)2(mpd)].2H2O [chel: chelidamate or 4-hydroxypyridine-2,6-dicarboxylate, mpd: 4-methylpyrimidine] was synthesized and characterized by single-crystal X-ray diffraction, UV-Vis and FT-IR spectroscopy. ...
A new chelidamate complex of nickel(II) ion, [Ni(chel)(H2O)2(mpd)].2H2O [chel: chelidamate or 4-hydroxypyridine-2,6-dicarboxylate, mpd: 4 …
Iodimetric determination of 2-mercaptopyrimidines.
Ciesielski W, Zakrzewski R, Krenc A, Zielinska J. Ciesielski W, et al. Talanta. 1998 Nov;47(3):745-52. doi: 10.1016/s0039-9140(98)00127-1. Talanta. 1998. PMID: 18967379
The determinability range in the volumetric titration, in phosphate buffer with starch as an indicator, was found to be equal to 40-1000 mumol for 2-mercaptopyrimidine (I) and 100-2000 mumol for 2-mercapto-4-methylpyrimidine (II), and 200-2000 mumol for 4,6-dimethyl …
The determinability range in the volumetric titration, in phosphate buffer with starch as an indicator, was found to be equal to 40-1000 mum …
Developing of N-(4-methylpyrimidine-2-yl)methacrylamide Langmuir-Blodgett thin film chemical sensor via quartz crystal microbalance technique.
Acikbas Y, Tetik GD, Ozkaya C, Bozkurt S, Capan R, Erdogan M. Acikbas Y, et al. Microsc Res Tech. 2020 Oct;83(10):1198-1207. doi: 10.1002/jemt.23511. Epub 2020 Jun 1. Microsc Res Tech. 2020. PMID: 32483896
In the present work, the characterization and gas sensing properties of newly synthesized N-(4-methylpyrimidine-2-yl)methacrylamide (N-MPMA) monomer Langmuir-Blodgett (LB) thin films were investigated. ...
In the present work, the characterization and gas sensing properties of newly synthesized N-(4-methylpyrimidine-2-yl)methacryl …
Effects of Both Methyl and Pyrimidine Groups in Fe-Ag Spin-Crossover Hofmann-Type Complex {Fe(4-Methylpyrimidine)(2)[Ag(CN)(2)](2)}.
Kitase K, Akahoshi D, Kitazawa T. Kitase K, et al. Inorg Chem. 2021 Apr 5;60(7):4717-4722. doi: 10.1021/acs.inorgchem.0c03655. Epub 2021 Mar 10. Inorg Chem. 2021. PMID: 33691406
This paper describes the synthesis of an Fe-Ag Hofmann-type complex, {Fe(4-methylpyrimidine)(2)[Ag(CN)(2)](2)}, which demonstrates a one-step SCO and single-layer Hofmann-type structure with Ag-N interactions and no Ag-Ag interactions, which is strikingly different …
This paper describes the synthesis of an Fe-Ag Hofmann-type complex, {Fe(4-methylpyrimidine)(2)[Ag(CN)(2)](2)}, which demonstr …
Bis(hfac)-copper(II) complexes bridged by pyrimidines showing magnetic interactions.
Yasui M, Ishikawa Y, Ishida T, Nogami T, Iwasaki F. Yasui M, et al. Acta Crystallogr B. 2001 Dec;57(Pt 6):772-9. doi: 10.1107/S0108768101013568. Epub 2001 Nov 29. Acta Crystallogr B. 2001. PMID: 11717476
Crystals of bis(1,1,1,5,5,5-hexafluoropentane-2,4-dionato)bispyrimidinecopper(II) (1), bis(1,1,1,5,5,5-hexafluoropentane-2,4-dionato)bis(4-methylpyrimidine)copper(II) (2), bis(1,1,1,5,5,5-hexafluoropentane-2,4-dionato)bis(quinazoline)copper(II) (3) showed ferromagne …
Crystals of bis(1,1,1,5,5,5-hexafluoropentane-2,4-dionato)bispyrimidinecopper(II) (1), bis(1,1,1,5,5,5-hexafluoropentane-2,4-dionato)bis( …
The recognition of diazinon, an organophosphorus pesticide, when found in samples in the form of decomposition products.
Sovocool GW, Harless RL, Bradway DE, Wright LH, Lores EM, Feige LE. Sovocool GW, et al. J Anal Toxicol. 1981 Mar-Apr;5(2):73-80. doi: 10.1093/jat/5.2.73. J Anal Toxicol. 1981. PMID: 7242025
The most abundant chemical compounds found in the sample included: 2-isopropyl-4-methyl-6-hydroxypyrimidine [2814-20-2]; 2-isopropyl-4-methyl-6-mercaptopyrimidine; 6,6'-dithiobis-(2-isopropyl-4-methylpyrimidine); 6,6'-dithiobis-(2-isopropyl-4-methylpyrimid …
The most abundant chemical compounds found in the sample included: 2-isopropyl-4-methyl-6-hydroxypyrimidine [2814-20-2]; 2-isopropyl-4-methy …
A novel two-step Fe-Au type spin-crossover behavior in a Hofmann-type coordination complex {Fe(4-methylpyrimidine)(2)[Au(CN)(2)](2)}.
Kitase K , Kitazawa T . Kitase K , et al. Dalton Trans. 2020 Sep 15;49(35):12210-12214. doi: 10.1039/d0dt01681k. Dalton Trans. 2020. PMID: 32608445
A Hofmann-type two-step spin-crossover (SCO) complex with a pyrimidine derivative ligand, Fe(4-methylpyrimidine)2[Au(CN)2]2, was synthesized, and this complex shows a two-step SCO phenomenon in the intermediate state. ...
A Hofmann-type two-step spin-crossover (SCO) complex with a pyrimidine derivative ligand, Fe(4-methylpyrimidine)2[Au(CN)2]2, w …
31 results