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Enantioselective Flow Synthesis of Rolipram Enabled by a Telescoped Asymmetric Conjugate Addition-Oxidative Aldehyde Esterification Sequence Using in Situ-Generated Persulfuric Acid as Oxidant.
Nagy BS, Llanes P, Pericas MA, Kappe CO, Ötvös SB. Nagy BS, et al. Org Lett. 2022 Feb 4;24(4):1066-1071. doi: 10.1021/acs.orglett.1c04300. Epub 2022 Jan 20. Org Lett. 2022. PMID: 35050638 Free PMC article.
The telescoped process takes advantage of a polystyrene-supported chiral organocatalyst along with in situ-generated persulfuric acid as a robust and scalable oxidant for direct aldehyde esterification. ...
The telescoped process takes advantage of a polystyrene-supported chiral organocatalyst along with in situ-generated persulfuric a
Harnessing a Continuous-Flow Persulfuric Acid Generator for Direct Oxidative Aldehyde Esterifications.
Nagy BS, Fu G, Hone CA, Kappe CO, Ötvös SB. Nagy BS, et al. ChemSusChem. 2023 Jan 20;16(2):e202201868. doi: 10.1002/cssc.202201868. Epub 2022 Dec 5. ChemSusChem. 2023. PMID: 36377674
Persulfuric acid is a well-known oxidant in various industrial-scale purification procedures. ...Sulfuric acid served as a readily available and benign precursor to form persulfuric acid in situ. ...
Persulfuric acid is a well-known oxidant in various industrial-scale purification procedures. ...Sulfuric acid served a
Total organic carbon analyzers as tools for measuring carbonaceous matter in natural waters.
Urbansky ET. Urbansky ET. J Environ Monit. 2001 Feb;3(1):102-12. doi: 10.1039/b006564l. J Environ Monit. 2001. PMID: 11253002 Review.
It provides a look into the fundamental principles and workings of TOC analyzers. Current peroxydisulfuric acid wet ashing methods and combustion methods are discussed. ...
It provides a look into the fundamental principles and workings of TOC analyzers. Current peroxydisulfuric acid wet ashing met …
Influence of cathode on the electro-generation of peroxydisulfuric acid oxidant and its application for effective removal of SO2 by room temperature electro-scrubbing process.
Balaji S, Muthuraman G, Moon IS. Balaji S, et al. J Hazard Mater. 2015 Dec 15;299:437-43. doi: 10.1016/j.jhazmat.2015.07.018. Epub 2015 Jul 14. J Hazard Mater. 2015. PMID: 26208110
Peroxydisulfuric acid oxidant (H2S2O8) was electro-generated using boron doped diamond (BDD) anode in an undivided electrolytic cell under the optimized conditions and used for the oxidative removal of gaseous SO2. ...The oxidative removal of SO2 in an electro-scrub
Peroxydisulfuric acid oxidant (H2S2O8) was electro-generated using boron doped diamond (BDD) anode in an undivided electrolyti
Direct analysis of oxidizing agents in aqueous solution with attenuated total reflectance mid-infrared spectroscopy and diamond-like carbon protected waveguides.
Janotta M, Vogt F, Voraberger HS, Waldhauser W, Lackner JM, Stotter C, Beutl M, Mizaikoff B. Janotta M, et al. Anal Chem. 2004 Jan 15;76(2):384-91. doi: 10.1021/ac034699d. Anal Chem. 2004. PMID: 14719887
IR microscopy was utilized to compare differences in the chemical surface modification of bare and protected ATR waveguides when exposed to hydrogen peroxide, peracetic acid, and peroxydisulfuric acid. The feasibility of DLC protected waveguides for real-time …
IR microscopy was utilized to compare differences in the chemical surface modification of bare and protected ATR waveguides when exposed to …