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Quoted phrases not found in phrase index: "dichlorosulfone", "sulfuric oxychloride", "sulfuryl dichloride"
Page 1
Direct Synthesis of Glycosyl Chlorides from Thioglycosides.
Hoard DJ, Sutar Y, Demchenko AV. Hoard DJ, et al. J Org Chem. 2024 May 17;89(10):6865-6876. doi: 10.1021/acs.joc.4c00244. Epub 2024 Apr 26. J Org Chem. 2024. PMID: 38669055 Free PMC article.
Reported herein is a new method for the direct synthesis of glycosyl chlorides from thioglycosides using sulfuryl chloride at rt. A variety of thioglycosides and thioimidates could be used as substrates. ...
Reported herein is a new method for the direct synthesis of glycosyl chlorides from thioglycosides using sulfuryl chloride at …
Regioselective synthesis of 2-aminophenols from N-arylhydroxylamines.
Gao Z, Hou Z, Gao H. Gao Z, et al. Org Biomol Chem. 2024 Oct 2;22(38):7801-7805. doi: 10.1039/d4ob01281j. Org Biomol Chem. 2024. PMID: 39252690
The 2-aminophenols were efficiently obtained through a cascade [3,3]-sigmatropic rearrangement and in situ hydrolysis process by using readily available N-arylhydroxylamines and the in situ-generated methyl chlorosulfonate from commercially available sulfuryl chloride …
The 2-aminophenols were efficiently obtained through a cascade [3,3]-sigmatropic rearrangement and in situ hydrolysis process by using readi …
Syntheses of 3',4',5,6-tetradioxyneamine and 5,6-dideoxyneamine.
Canas-Rodriguez A, Ruiz-Poveda SG. Canas-Rodriguez A, et al. Carbohydr Res. 1977 Oct;58(2):379-85. doi: 10.1016/s0008-6215(00)84364-5. Carbohydr Res. 1977. PMID: 912693
3',4',5,6-Tetradoxyneamine (7) was synthesized from neamine by the reaction sequence N-acetylation, O-mesylation, treatment with sodium iodide-zinc dust, hydrogenation, and base hyrolysis, Alternatively, 7 was obtained by treatment of tetra-(N-methoxycarbonyl)neamine with sulp …
3',4',5,6-Tetradoxyneamine (7) was synthesized from neamine by the reaction sequence N-acetylation, O-mesylation, treatment with sodium iodi …
Development of a derivatization RP-HPLC method for determination of sulfuryl chloride in chlorosulfonic acid for gefapixant citrate manufacture.
Huang C, Song S, Liu W, Parganiha P, Zhuang P, Lohani S, Alwedi E, Ren H, Bishara D, Chang HYD. Huang C, et al. J Pharm Biomed Anal. 2022 Jun 5;215:114752. doi: 10.1016/j.jpba.2022.114752. Epub 2022 Apr 4. J Pharm Biomed Anal. 2022. PMID: 35483232
Various direct analysis methods were evaluated and found unsuitable because of the highly reactive nature and structural similarity of sulfuryl chloride and CSA. Therefore, a robust derivatization reversed-phase high performance liquid chromatography (RP-HPLC) metho …
Various direct analysis methods were evaluated and found unsuitable because of the highly reactive nature and structural similarity of su …
Reactions of enantiopure cyclic diols with sulfuryl chloride.
Boyd DR, Sharma ND, Kaik M, McIntyre PB, Malone JF, Stevenson PJ. Boyd DR, et al. Org Biomol Chem. 2014 Apr 7;12(13):2128-36. doi: 10.1039/c4ob00042k. Epub 2014 Feb 26. Org Biomol Chem. 2014. PMID: 24569926
Monocyclic allylic cis-1,2-diols reacted with sulfuryl chloride at 0 C in a regio- and stereo-selective manner to give 2-chloro-1-sulfochloridates, which were hydrolysed to yield the corresponding trans-1,2-chlorohydrins. At -78 C, with very slow addition of su …
Monocyclic allylic cis-1,2-diols reacted with sulfuryl chloride at 0 C in a regio- and stereo-selective manner to give 2-chlo …
A charring method for quantitative determination of carbohydrates on thin-layer chromatograms.
Robin J, Bernard J. Robin J, et al. Exp Biol. 1986;45(2):123-6. Exp Biol. 1986. PMID: 3699130
The method is based on charring the spots with sulphuric acid generated from interaction of sulphuryl chloride with water vapour, and quantification of carbohydrates by photodensitometry of the chromatograms. ...
The method is based on charring the spots with sulphuric acid generated from interaction of sulphuryl chloride with water vapo …
Amine organocatalysts for highly ortho-selective chlorination of anilines with sulfuryl chloride.
Wang X, Chen Z, Liu Q, Lin W, Xiong X. Wang X, et al. Chem Commun (Camb). 2022 Dec 1;58(96):13325-13328. doi: 10.1039/d2cc05320a. Chem Commun (Camb). 2022. PMID: 36325927
A metal catalyst free approach for regioselective ortho-chlorination of anilines has been developed using a secondary amine as the organocatalyst and sulfuryl chloride as the halogen source under mild conditions. A wide range of substrates were compatible with this …
A metal catalyst free approach for regioselective ortho-chlorination of anilines has been developed using a secondary amine as the organocat …
Transformations of cellobiose derivatives into analogues of lactose.
Edwards RG, Hough L, Richardson AC. Edwards RG, et al. Carbohydr Res. 1977 May;55:129-48. doi: 10.1016/s0008-6215(00)84450-x. Carbohydr Res. 1977. PMID: 861973
In addition, reaction of the pentabenzoate 2b with sulphuryl chloride initially afforded the 6'-chloro derivative, which was then slowly transformed into a mixture of the 4',6'-dichloro-lactoside and an isomer in which the non-reducing ring of the disaccharide had b …
In addition, reaction of the pentabenzoate 2b with sulphuryl chloride initially afforded the 6'-chloro derivative, which was t …
57 results