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Page 1
Synthesis of 1-formyldipyrromethanes.
Ptaszek M, McDowell BE, Lindsey JS. Ptaszek M, et al. J Org Chem. 2006 May 26;71(11):4328-31. doi: 10.1021/jo060119b. J Org Chem. 2006. PMID: 16709082
Two methods of synthesis of 1-formyldipyrromethanes have been investigated: (1) Vilsmeier formylation followed by selective removal of the unwanted 1,9-diformyldipyrromethane by dialkyltin complexation and (2) reaction with mesitylmagnesium bromide (MesMgBr) followed by formylati …
Two methods of synthesis of 1-formyldipyrromethanes have been investigated: (1) Vilsmeier formylation followed by selective removal of the u …
Nickel-Catalyzed Asymmetric Hydroaryloxy- and Hydroalkoxycarbonylation of Cyclopropenes.
Yu R, Cai SZ, Li C, Fang X. Yu R, et al. Angew Chem Int Ed Engl. 2022 Sep 5;61(36):e202200733. doi: 10.1002/anie.202200733. Epub 2022 Jul 26. Angew Chem Int Ed Engl. 2022. PMID: 35836371
Here we report a nickel-catalyzed asymmetric carbonylation of cyclopropenes with phenyl formate and CO/ROH, respectively. This asymmetrical synthetic protocol features high atom economy, good functional group tolerance, which rapidly constructs polysubstituted cyclo …
Here we report a nickel-catalyzed asymmetric carbonylation of cyclopropenes with phenyl formate and CO/ROH, respectively. This …
What a difference a chlorine makes: The remarkable unimolecular ion chemistry of phenyl formate and phenyl chloroformate.
Lowe B, Cardona AL, Salas J, Bodi A, Mayer PM, Burgos Paci MA. Lowe B, et al. J Mass Spectrom. 2024 Feb;59(2):e5004. doi: 10.1002/jms.5004. J Mass Spectrom. 2024. PMID: 38311470
Imaging photoelectron photoion coincidence (iPEPICO) spectroscopy and tandem mass spectrometry were employed to explore the ionisation and dissociative ionisation of phenyl formate (PF) and phenyl chloroformate (PCF). The threshold photoelectron spectra of both comp …
Imaging photoelectron photoion coincidence (iPEPICO) spectroscopy and tandem mass spectrometry were employed to explore the ionisation and d …
Creation of Novel Toxic Gas Surrogates and the Development of Safe and Facile Catalytic Reactions.
Konishi H. Konishi H. Chem Pharm Bull (Tokyo). 2018;66(1):1-19. doi: 10.1248/cpb.c17-00795. Chem Pharm Bull (Tokyo). 2018. PMID: 29311504 Free article. Review.
Improvements in substrate scope during the hydroesterification of alkenes using formates facilitated by the Ru-imidazole catalyst system provided the opportunity to discover that phenyl formate is a useful carbon monoxide (CO) surrogate for the generation of CO and …
Improvements in substrate scope during the hydroesterification of alkenes using formates facilitated by the Ru-imidazole catalyst system pro …
Microhydration of Phenyl Formate: Gas-Phase Laser Spectroscopy, Microwave Spectroscopy, and Quantum Chemistry Calculations.
Panwaria P, Juanes M, Mishra KK, Saragi R, Borish K, Usabiaga I, Camiruaga A, Fernández JA, Lesarri A, Das A. Panwaria P, et al. Chemphyschem. 2022 Dec 16;23(24):e202200330. doi: 10.1002/cphc.202200330. Epub 2022 Sep 6. Chemphyschem. 2022. PMID: 35984348
Herein, we have investigated the structure of phenyl formate water (PhOF H(2) O) dimer and various non-covalent interactions present there using gas-phase laser spectroscopy and microwave spectroscopy combined with quantum chemistry calculations. ...
Herein, we have investigated the structure of phenyl formate water (PhOF H(2) O) dimer and various non-covalent interactio …
Nickel/Photoredox-Catalyzed Carbonylative Cross-Electrophile Coupling of Organohalides and Carboxylic Acid Esters with Phenyl Formate.
Yan XB, Wang N, Zhou J, Ge H, Wang Z, Lin Y, Shui H. Yan XB, et al. Org Lett. 2024 Aug 2;26(30):6518-6522. doi: 10.1021/acs.orglett.4c02502. Epub 2024 Jul 22. Org Lett. 2024. PMID: 39038071
A photoinduced nickel-catalyzed reductive carbonylative coupling from organohalides and N-(acyloxy)phthalimide esters with phenyl formate as the carbonyl source has been developed. This reaction could perform smoothly under mild conditions, and a series of aryl-alky …
A photoinduced nickel-catalyzed reductive carbonylative coupling from organohalides and N-(acyloxy)phthalimide esters with phenyl …
First homoleptic complexes of isocyanoferrocene.
Barybin MV, Holovics TC, Deplazes SF, Lushington GH, Powell DR, Toriyama M. Barybin MV, et al. J Am Chem Soc. 2002 Nov 20;124(46):13668-9. doi: 10.1021/ja028271s. J Am Chem Soc. 2002. PMID: 12431084
Interaction of aminoferrocene with a 65/35 mol % mixture of phenyl formate/phenol followed by subsequent dehydration of the resulting ferrocenylformamide with POCl3 produced a high yield of air- and thermally stable, peach-colored isocyanoferrocene (CNFc). ...
Interaction of aminoferrocene with a 65/35 mol % mixture of phenyl formate/phenol followed by subsequent dehydration of the re …
Palladium-Catalyzed Highly Regio- and Enantioselective Hydroesterification of Aryl Olefins with Phenyl Formate.
Li J, Chang W, Ren W, Dai J, Shi Y. Li J, et al. Org Lett. 2016 Nov 4;18(21):5456-5459. doi: 10.1021/acs.orglett.6b02467. Epub 2016 Oct 25. Org Lett. 2016. PMID: 27779413
An effective Pd-catalyzed regio- and enantioselective hydroesterification of aryl olefins with phenyl formate is described. A variety of phenyl 2-arylpropanoates can be obtained in good yields with high b/l ratios and ee's without using toxic CO gas....
An effective Pd-catalyzed regio- and enantioselective hydroesterification of aryl olefins with phenyl formate is described. A …
Palladium-catalyzed carbonylative synthesis of isocoumarins and phthalides by using phenyl formate as a carbon monoxide source.
Yuan Q, Chen ZB, Zhang FL, Zhu YM. Yuan Q, et al. Org Biomol Chem. 2017 Feb 21;15(7):1628-1635. doi: 10.1039/c6ob02409b. Epub 2017 Jan 25. Org Biomol Chem. 2017. PMID: 28120978
A simple and efficient palladium-catalyzed intramolecular carbonylative synthesis of isocoumarins and phthalides from the easily available starting materials by employing phenyl formate as a CO surrogate has been achieved. The approach affords target compounds in go …
A simple and efficient palladium-catalyzed intramolecular carbonylative synthesis of isocoumarins and phthalides from the easily available s …
35 results