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Scalable synthesis of 5,11-diethynylated indeno[1,2-b]fluorene-6,12-diones and exploration of their solid state packing.
Rose BD, Santa Maria PJ, Fix AG, Vonnegut CL, Zakharov LN, Parkin SR, Haley MM. Rose BD, et al. Among authors: vonnegut cl. Beilstein J Org Chem. 2014 Sep 5;10:2122-30. doi: 10.3762/bjoc.10.219. eCollection 2014. Beilstein J Org Chem. 2014. PMID: 25246970 Free PMC article.
We report a new synthetic route to 5,11-disubstituted indeno[1,2-b]fluorene-6,12-diones that is amenable to larger scale reactions, allowing for the preparation of gram amounts of material. With this new methodology, we explored the effects on crystal packing morphology fo …
We report a new synthetic route to 5,11-disubstituted indeno[1,2-b]fluorene-6,12-diones that is amenable to larger scale reactions, a …