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Page 1
Chains or rings? Polymorphism of an isoniazid derivative derivatized with diacetone alcohol.
Scheepers MC, Fernandes MA, Lemmerer A. Scheepers MC, et al. RSC Adv. 2022 Apr 14;12(19):11658-11664. doi: 10.1039/d2ra02057b. eCollection 2022 Apr 13. RSC Adv. 2022. PMID: 35432943 Free PMC article.
Isoniazid was derivated with diacetone alcohol in a Schiff-base reaction in order to yield N'-[(2E)-4-hydroxy-4-methylpentan-2-ylidene]pyridine-4-carbohydrazide. ...
Isoniazid was derivated with diacetone alcohol in a Schiff-base reaction in order to yield N'-[(2E)-4-hydroxy-4-methylpentan-2 …
Aldol condensation of refluxing acetone on CaC(2) achieves efficient coproduction of diacetone alcohol, mesityl oxide and isophorone.
Xu X, Meng H, Lu Y, Li C. Xu X, et al. RSC Adv. 2018 Aug 30;8(53):30610-30615. doi: 10.1039/c8ra05965a. eCollection 2018 Aug 24. RSC Adv. 2018. PMID: 35546820 Free PMC article.
Efficient production of diacetone alcohol (DAA), mesityl oxide (MO) and isophorone (IP) is important for the high value utilization of acetone. ...
Efficient production of diacetone alcohol (DAA), mesityl oxide (MO) and isophorone (IP) is important for the high value utiliz …
Roles of acetone and diacetone alcohol in coordination and dissociation reactions of uranyl complexes.
Rios D, Schoendorff G, Van Stipdonk MJ, Gordon MS, Windus TL, Gibson JK, de Jong WA. Rios D, et al. Inorg Chem. 2012 Dec 3;51(23):12768-75. doi: 10.1021/ic3015964. Epub 2012 Nov 12. Inorg Chem. 2012. PMID: 23146003
Combined collision-induced dissociation mass spectrometry experiments with DFT and MP2 calculations were employed to elucidate the molecular structures and energetics of dissociation reactions of uranyl species containing acetone and diacetone alcohol ligands. It is …
Combined collision-induced dissociation mass spectrometry experiments with DFT and MP2 calculations were employed to elucidate the molecular …
Analysis of thermolabile residual solvents in a spray dried dispersion using static headspace gas chromatography.
Oliveira A, Bambrick ST, Pfund LY, Diamandopoulos P, Gong X, Liang X, Mowery MD, Zheng J. Oliveira A, et al. J Sep Sci. 2019 Mar;42(6):1222-1229. doi: 10.1002/jssc.201801024. Epub 2019 Jan 22. J Sep Sci. 2019. PMID: 30618204
In this study, we discuss the development of a static headspace gas chromatography method for the analysis of residual acetone as well as its enriched impurities including mesityl oxide and diacetone alcohol, in a spray dried dispersion. The major challenges include …
In this study, we discuss the development of a static headspace gas chromatography method for the analysis of residual acetone as well as it …
Acetone Factor in the Design of Cu4-, Cu6-, and Cu9-Based Cage Coppersilsesquioxanes: Synthesis, Structural Features, and Catalytic Functionalization of Alkanes.
Bilyachenko AN, Gutsul EI, Khrustalev VN, Astakhov GS, Zueva AY, Zubavichus YV, Kirillova MV, Shul'pina LS, Ikonnikov NS, Dorovatovskii PV, Shubina ES, Kirillov AM, Shul'pin GB. Bilyachenko AN, et al. Inorg Chem. 2022 Sep 19;61(37):14800-14814. doi: 10.1021/acs.inorgchem.2c02217. Epub 2022 Sep 4. Inorg Chem. 2022. PMID: 36059209
A heterometallic Cu(4)Na(4)-sandwich-like derivative represents the first example of a metallasilsesquioxane complex with diacetone alcohol ligands formed in situ due to acetone condensation reaction. ...
A heterometallic Cu(4)Na(4)-sandwich-like derivative represents the first example of a metallasilsesquioxane complex with diacetone
Diacetone alcohol, a dispersant solvent, contributes to acute toxicity of a fipronil-based insecticide in a passerine bird.
Kitulagodage M, Astheimer LB, Buttemer WA. Kitulagodage M, et al. Ecotoxicol Environ Saf. 2008 Oct;71(2):597-600. doi: 10.1016/j.ecoenv.2007.11.001. Epub 2007 Dec 21. Ecotoxicol Environ Saf. 2008. PMID: 18155147
Under laboratory conditions, we identified unexpectedly high toxicities due exclusively to diacetone alcohol (DAA), a solvent making up 12.5% of the Adonis 3UL formulation. ...
Under laboratory conditions, we identified unexpectedly high toxicities due exclusively to diacetone alcohol (DAA), a solvent …
Trace Level Determination of Mesityl Oxide and Diacetone Alcohol in Atazanavir Sulfate Drug Substance by a Gas Chromatography Method.
Raju KV, Pavan Kumar KS, Siva Krishna N, Madhava Reddy P, Sreenivas N, Kumar Sharma H, Himabindu G, Annapurna N. Raju KV, et al. Sci Pharm. 2016 Apr-Jun;84(2):321-31. doi: 10.3797/scipharm.1507-05. Epub 2015 Aug 27. Sci Pharm. 2016. PMID: 27222607 Free PMC article.
The detection and quantitation limits obtained for mesityl oxide and diacetone alcohol were 5 g/g and 10 g/g, respectively, for both of the analytes. The method was found to be linear in the range between 10 g/g and 150 g/g with a correlation coefficient greater tha …
The detection and quantitation limits obtained for mesityl oxide and diacetone alcohol were 5 g/g and 10 g/g, respectively, fo …
Rate and grade transition control using PI controller based supervisory and regulatory layers: Diacetone alcohol process case study.
Srivastava S, Bhartiya S. Srivastava S, et al. ISA Trans. 2022 Sep;128(Pt B):287-293. doi: 10.1016/j.isatra.2021.11.001. Epub 2021 Nov 23. ISA Trans. 2022. PMID: 34861986
The PI based supervisory-regulatory control structure is illustrated using simulated case studies on a prototypical process for diacetone alcohol production comprising of a reactor followed by two distillation columns and a recycle....
The PI based supervisory-regulatory control structure is illustrated using simulated case studies on a prototypical process for diacetone
Structure Revision of Penipacids A-E Reveals a Putative New Cryptic Natural Product, N-aminoanthranilic Acid, with Potential as a Transcriptional Regulator of Silent Secondary Metabolism.
Khalil ZG, Kankanamge S, Capon RJ. Khalil ZG, et al. Mar Drugs. 2022 May 24;20(6):339. doi: 10.3390/md20060339. Mar Drugs. 2022. PMID: 35736142 Free PMC article. Review.
This revision strongly supported the proposition that penipacids A-B (6-7) were artifact Schiff base adducts of the cryptic (undetected) natural product N-aminoanthranilic acid (11) with diacetone alcohol, induced by excessive exposure to acetone and methanol under …
This revision strongly supported the proposition that penipacids A-B (6-7) were artifact Schiff base adducts of the cryptic (undetected) nat …
48 results