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Through the looking glass--a new world of proteins enabled by chemical synthesis.
Kent S, Sohma Y, Liu S, Bang D, Pentelute B, Mandal K. Kent S, et al. J Pept Sci. 2012 Jul;18(7):428-36. doi: 10.1002/psc.2421. Epub 2012 Jun 4. J Pept Sci. 2012. PMID: 22674813 Review.
Inversion of the Side-Chain Stereochemistry of Indvidual Thr or Ile Residues in a Protein Molecule: Impact on the Folding, Stability, and Structure of the ShK Toxin.
Dang B, Shen R, Kubota T, Mandal K, Bezanilla F, Roux B, Kent SB. Dang B, et al. Angew Chem Int Ed Engl. 2017 Mar 13;56(12):3324-3328. doi: 10.1002/anie.201612398. Epub 2017 Feb 14. Angew Chem Int Ed Engl. 2017. PMID: 28194851 Free PMC article.
Crystal structure of chemically synthesized HIV-1 protease and a ketomethylene isostere inhibitor based on the p2/NC cleavage site.
Torbeev VY, Mandal K, Terechko VA, Kent SB. Torbeev VY, et al. Bioorg Med Chem Lett. 2008 Aug 15;18(16):4554-7. doi: 10.1016/j.bmcl.2008.07.039. Epub 2008 Jul 15. Bioorg Med Chem Lett. 2008. PMID: 18657969
Reprint of "Crystal structure of chemically synthesized HIV-1 protease and a ketomethylene isostere inhibitor based on the p2/NC cleavage site" [Bioorg. Med. Chem. Lett. 18 (2008) 4554-4557].
Torbeev VY, Mandal K, Terechko VA, Kent SB. Torbeev VY, et al. Bioorg Med Chem Lett. 2008 Nov 15;18(22):6012-5. doi: 10.1016/S0960-894X(08)01314-0. Bioorg Med Chem Lett. 2008. PMID: 18995173
Total chemical synthesis and X-ray structure of kaliotoxin by racemic protein crystallography.
Pentelute BL, Mandal K, Gates ZP, Sawaya MR, Yeates TO, Kent SB. Pentelute BL, et al. Chem Commun (Camb). 2010 Nov 21;46(43):8174-6. doi: 10.1039/c0cc03148h. Epub 2010 Sep 28. Chem Commun (Camb). 2010. PMID: 20877851
Crystallization of Enantiomerically Pure Proteins from Quasi-Racemic Mixtures: Structure Determination by X-Ray Diffraction of Isotope-Labeled Ester Insulin and Human Insulin.
Mandal K, Dhayalan B, Avital-Shmilovici M, Tokmakoff A, Kent SB. Mandal K, et al. Chembiochem. 2016 Mar 2;17(5):421-5. doi: 10.1002/cbic.201500600. Epub 2016 Feb 10. Chembiochem. 2016. PMID: 26707939
(Quasi-)racemic X-ray structures of glycosylated and non-glycosylated forms of the chemokine Ser-CCL1 prepared by total chemical synthesis.
Okamoto R, Mandal K, Sawaya MR, Kajihara Y, Yeates TO, Kent SB. Okamoto R, et al. Angew Chem Int Ed Engl. 2014 May 12;53(20):5194-8. doi: 10.1002/anie.201400679. Epub 2014 Apr 1. Angew Chem Int Ed Engl. 2014. PMID: 24692304
A functional role of Rv1738 in Mycobacterium tuberculosis persistence suggested by racemic protein crystallography.
Bunker RD, Mandal K, Bashiri G, Chaston JJ, Pentelute BL, Lott JS, Kent SB, Baker EN. Bunker RD, et al. Proc Natl Acad Sci U S A. 2015 Apr 7;112(14):4310-5. doi: 10.1073/pnas.1422387112. Epub 2015 Mar 23. Proc Natl Acad Sci U S A. 2015. PMID: 25831534 Free PMC article.
Scope and Limitations of Fmoc Chemistry SPPS-Based Approaches to the Total Synthesis of Insulin Lispro via Ester Insulin.
Dhayalan B, Mandal K, Rege N, Weiss MA, Eitel SH, Meier T, Schoenleber RO, Kent SB. Dhayalan B, et al. Chemistry. 2017 Jan 31;23(7):1709-1716. doi: 10.1002/chem.201605578. Epub 2017 Jan 10. Chemistry. 2017. PMID: 27905149 Free PMC article.
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