Scrophularia Tenuipes Coss and Durieu: Phytochemical Composition and Biological Activities

Molecules. 2020 Apr 3;25(7):1647. doi: 10.3390/molecules25071647.

Abstract

Scrophularia tenuipes is an Algerian-Tunisian endemic species, which has not been studied yet. Ethyl acetate (EA) and n-butanol (Bu) fractions obtained from Scrophularia tenuipes were investigated for their health benefit properties, in particular with respect to in vivo/in vitro anti-inflammatory and antioxidant activities, as well as their potential to inhibit key enzymes with impact in diabetes (α-glucosidase and α-amylase). The fractions had a distinct phytochemical composition, of which EA was richer in total phenolic compounds (225 mg GAE/g) and mostly composed of the phenylethanoid acetyl martynoside. Compared to EA, Bu had higher amounts of total flavonoids, and according to the result obtained from UHPLC-DAD-ESI-MSn analysis, harpagoside (iridoid) was its major phytochemical. EA fraction was quite promising with regard to the in vivo (at 200 mg/kg, po) anti-inflammatory effect (62% and 52% for carrageenan-induced rat paw edema and xylene-induced ear edema tests, respectively), while Bu fraction exhibited a stronger antioxidant capacity in all tests (IC50 = 68 µg/mL, IC50 = 18 µg/mL, IC50 = 18 µg/mL and A0.50 = 43 µg/mL for DPPH, ABTS•+, O2•- scavenging assays and cupric-reducing antioxidant capacity method, respectively). Both fractions also showed a strong effect against α-amylase enzyme (IC50 = 8 µg/mL and 10 µg/mL for EA and Bu fraction, respectively).

Keywords: Scrophularia tenuipes; UHPLC-ESI-DAD-MSn; anti-inflammatory; antidiabetic; antioxidant; iridoids; phenolic; phenylethanoid.

MeSH terms

  • 1-Butanol / chemistry
  • Acetates / chemistry
  • Animals
  • Anti-Inflammatory Agents / administration & dosage*
  • Anti-Inflammatory Agents / chemistry
  • Anti-Inflammatory Agents / isolation & purification
  • Anti-Inflammatory Agents / pharmacology
  • Antioxidants / administration & dosage*
  • Antioxidants / chemistry
  • Antioxidants / isolation & purification
  • Antioxidants / pharmacology
  • Carrageenan / adverse effects
  • Edema / chemically induced
  • Edema / drug therapy*
  • Female
  • Flavonoids / chemistry
  • Flavonoids / isolation & purification
  • Flavonoids / pharmacology
  • Free Radicals / chemistry
  • Phytochemicals / administration & dosage*
  • Phytochemicals / chemistry
  • Phytochemicals / isolation & purification
  • Phytochemicals / pharmacology
  • Rats
  • Scrophularia / chemistry*
  • Xylenes / adverse effects

Substances

  • Acetates
  • Anti-Inflammatory Agents
  • Antioxidants
  • Flavonoids
  • Free Radicals
  • Phytochemicals
  • Xylenes
  • ethyl acetate
  • 1-Butanol
  • Carrageenan