Evaluation of Radiopacity of Luting Cements Submitted to Different Aging Procedures

J Prosthodont. 2018 Dec;27(9):853-859. doi: 10.1111/jopr.12989. Epub 2018 Oct 28.

Abstract

Purpose: To evaluate the radiopacity of luting cements submitted to different aging procedures.

Materials and methods: Twenty discs (1 × 4 mm) of each of the following cements were prepared: zinc phosphate, RelyX Luting 2, Variolink 2, AllCem, RelyX U200, Multilink, Panavia F2.0, and RelyX ARC. Then, they were randomly divided into two groups (n = 10/group), according to the aging procedure: thermal cycling group and water storage group. Before and after aging procedures, specimens were x-rayed with an aluminum step-wedge (11 steps, 1 mm thick each) and three dental slices (1 mm thick). The radiopacity was evaluated by means of optical density, which was measured using ImageJ software. The values were converted into millimeters of aluminum with a logistic regression calibration curve. The data were analyzed by one-way ANOVA and Tukey post-hoc test (α = 0.05).

Results: In the thermal cycling group, RelyX Luting 2, RelyX U200, and Panavia F2.0 showed a statistically significant reduction in radiopacity (p < 0.05). In the water storage group, all cements showed a significant reduction in radiopacity (p < 0.05), and RelyX Luting 2 and Panavia F2.0 performed below the desired ISO 4049 standard.

Conclusions: The radiopacity of luting cements can decrease after aging, especially after 1-year water storage.

Keywords: Dental digital radiography; resin cements; thermal cycling.

MeSH terms

  • Composite Resins / adverse effects
  • Composite Resins / chemistry
  • Dental Cements / adverse effects*
  • Dental Cements / chemistry
  • Glass Ionomer Cements / adverse effects
  • Glass Ionomer Cements / chemistry
  • Humans
  • Optical Phenomena
  • Radiography, Dental
  • Resin Cements / adverse effects
  • Resin Cements / chemistry

Substances

  • Composite Resins
  • Dental Cements
  • Glass Ionomer Cements
  • Panavia-Fluoro
  • RelyX U200
  • Resin Cements
  • Vitremer