Mussel-Inspired Polymeric Coatings to Realize Functions from Single and Dual to Multiple Antimicrobial Mechanisms

ACS Appl Mater Interfaces. 2021 Jan 20;13(2):3089-3097. doi: 10.1021/acsami.0c16510. Epub 2021 Jan 5.

Abstract

Numerous efforts to fabricate antimicrobial surfaces by simple yet universal protocols with high efficiency have attracted considerable interest but proved to be particularly challenging. Herein, we designed and fabricated a series of antimicrobial polymeric coatings with different functions from single to multiple mechanisms by selectively utilizing diethylene glycol diglycidyl ether (PEGDGE), polylysine, and poly[glycidylmethacrylate-co-3-(dimethyl(4-vinylbenzyl)ammonium)propyl sulfonate] (poly(GMA-co-DVBAPS)) via straightforward mussel-inspired codeposition techniques. Bactericidal polylysine endowed the modified surfaces with a high ability (∼90%) to kill attached bacteria, while PEGDGE components with unique surface hydration prevented bacterial adhesion, avoiding the initial biofilm formation. Moreover, excellent salt-responsive poly(GMA-co-DVBAPS) enabled reactant polymeric coatings to change chain conformations from shrinkable to stretchable state and subsequently release >90% attached bacteria when treated with NaCl solution, even after repeated cycles. Therefore, the obtained polymeric coatings, polydopamine/poly(GMA-co-DVBAPS) (PDA/PDV), polydopamine/polylysine/poly(GMA-co-DVBAPS) (PDA/l-PDV), and polydopamine/polylysine/poly(GMA-co-DVBAPS)/diethylene glycol diglycidyl ether (PDA/l-PDV-PEGDGE), controllably realized functions from single and dual to multiple antimicrobial mechanisms, as evidenced by long-term antifouling activity to bacteria, high bactericidal efficiency, and salt-responsive bacterial regeneration performance with several bacterial killing-release cycles. This study not only contributes to mussel-inspired chemistry for polymeric coatings with controllable functions but also provides a series of reliable and highly efficient antimicrobial surfaces for potential biomedical applications.

Keywords: antifouling; antimicrobial material; mussel-inspired chemistry; polymeric coating; salt-responsive.

MeSH terms

  • Animals
  • Anti-Bacterial Agents / chemistry*
  • Anti-Bacterial Agents / pharmacology*
  • Bacterial Adhesion / drug effects
  • Bacterial Infections / microbiology
  • Bacterial Infections / prevention & control
  • Biomimetic Materials / chemistry
  • Biomimetic Materials / pharmacology
  • Bivalvia / chemistry
  • Coated Materials, Biocompatible / chemistry*
  • Coated Materials, Biocompatible / pharmacology*
  • Escherichia coli / drug effects
  • Escherichia coli / physiology
  • Ethylene Glycols / chemistry
  • Ethylene Glycols / pharmacology
  • Humans
  • Indoles / chemistry
  • Indoles / pharmacology
  • Polylysine / chemistry
  • Polylysine / pharmacology
  • Polymers / chemistry*
  • Polymers / pharmacology*
  • Polymethacrylic Acids / chemistry
  • Polymethacrylic Acids / pharmacology
  • Staphylococcus aureus / drug effects
  • Staphylococcus aureus / physiology
  • Surface Properties

Substances

  • Anti-Bacterial Agents
  • Coated Materials, Biocompatible
  • Ethylene Glycols
  • Indoles
  • Polymers
  • Polymethacrylic Acids
  • polydopamine
  • Polylysine