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Discovery of two clinical histamine H(3) receptor antagonists: trans-N-ethyl-3-fluoro-3-[3-fluoro-4-(pyrrolidinylmethyl)phenyl]cyclobutanecarboxamide (PF-03654746) and trans-3-fluoro-3-[3-fluoro-4-(pyrrolidin-1-ylmethyl)phenyl]-N-(2-methylpropyl)cyclobutanecarboxamide (PF-03654764).
Wager TT, Pettersen BA, Schmidt AW, Spracklin DK, Mente S, Butler TW, Howard H, Lettiere DJ, Rubitski DM, Wong DF, Nedza FM, Nelson FR, Rollema H, Raggon JW, Aubrecht J, Freeman JK, Marcek JM, Cianfrogna J, Cook KW, James LC, Chatman LA, Iredale PA, Banker MJ, Homiski ML, Munzner JB, Chandrasekaran RY. Wager TT, et al. Among authors: raggon jw. J Med Chem. 2011 Nov 10;54(21):7602-20. doi: 10.1021/jm200939b. Epub 2011 Oct 7. J Med Chem. 2011. PMID: 21928839
Pharmaceutical impurity identification: a case study using a multidisciplinary approach.
Alsante KM, Boutros P, Couturier MA, Friedmann RC, Harwood JW, Horan GJ, Jensen AJ, Liu Q, Lohr LL, Morris R, Raggon JW, Reid GL, Santafianos DP, Sharp TR, Tucker JL, Wilcox GE. Alsante KM, et al. Among authors: raggon jw. J Pharm Sci. 2004 Sep;93(9):2296-309. doi: 10.1002/jps.20120. J Pharm Sci. 2004. PMID: 15295790