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A New JECFA Method for GC-MS Determination of Propylene Chlorohydrine Residues in Hydroxypropylated Starches.
van der Ark M, Hopman J, Mijland P, Mulder W, Asdarci F, O'Connell X, Medic J, Wei Q, Brunt K. van der Ark M, et al. J AOAC Int. 2023 Sep 1;106(5):1220-1229. doi: 10.1093/jaoacint/qsad042. J AOAC Int. 2023. PMID: 37027229
RESULTS: This single-laboratory validation (SLV) study showed good linear calibrations for both 1-chloro-2-propanol (PCH-1) and 2-chloro-1-propanol (PCH-2) in the concentration range of 0.5-4 mg/kg in dry starch. ...
RESULTS: This single-laboratory validation (SLV) study showed good linear calibrations for both 1-chloro-2-propanol (PCH-1) and 2- …
NTP Toxicology and Carcinogenesis Studies of 1-Chloro-2-propanol (Technical Grade) (CAS NO. 127-00-4) in F344/N Rats and B6C3F1 Mice (Drinking Water Studies.
National Toxicology Program. National Toxicology Program. Natl Toxicol Program Tech Rep Ser. 1998 Sep;477:1-264. Natl Toxicol Program Tech Rep Ser. 1998. PMID: 12571686 Free article.
1-Chloro-2-propanol and its positional isomer, 2-chloro-1-propanol, are used as chemical intermediates for the manufacture of propylene oxide, a starting material for production of polyurethane polyols and propylene glycol. ...Male and female F344/N ra …
1-Chloro-2-propanol and its positional isomer, 2-chloro-1-propanol, are used as chemical intermediates for the m …
Elimination of N,O-bis(trimethylsilyl)trifluoroacetamide interference by base treatment in derivatization gas chromatography mass spectrometry determination of parts per billion of alcohols in a food additive.
Zhu K, Gu B, Kerry M, Mintert M, Luong J, Pursch M. Zhu K, et al. J Chromatogr A. 2017 Mar 24;1490:74-79. doi: 10.1016/j.chroma.2017.02.025. Epub 2017 Feb 14. J Chromatogr A. 2017. PMID: 28238325
A novel base treatment followed by liquid-liquid extraction was developed to remove the interference of excess derivatization reagent BSTFA [N,O-Bis(trimethylsilyl)trifluoroacetamide] and its byproducts for trace determination of 1-chloro-2-propanol and 2-chloro- …
A novel base treatment followed by liquid-liquid extraction was developed to remove the interference of excess derivatization reagent BSTFA …
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