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Toxicology studies of allyl bromide (CAS No. 106-95-6) in genetically modified (FVB Tg.AC hemizygous) mice and carcinogenicity studies of allyl bromide in genetically modified [B6.129-Trp53tm1Brd (N5) Haploinsufficient] mice (dermal and gavage studies).
National Toxicology Program. National Toxicology Program. Natl Toxicol Program Genet Modif Model Rep. 2008 Apr;(7):1-122. Natl Toxicol Program Genet Modif Model Rep. 2008. PMID: 18784760 Free PMC article.
It has been described as an insecticidal fumigant used in crop protection. Male and female FVB/N and C57BL/6 mice received allyl bromide (greater than 99% pure) by gavage and dermal application, respectively, for 2 weeks, and FVB/N, C57BL/6, Tg.AC hemizygous, and p5 …
It has been described as an insecticidal fumigant used in crop protection. Male and female FVB/N and C57BL/6 mice received allyl b …
Indium-Mediated Stereoselective Allylation.
Kumar D, Vemula SR, Balasubramanian N, Cook GR. Kumar D, et al. Acc Chem Res. 2016;49(10):2169-2178. doi: 10.1021/acs.accounts.6b00362. Epub 2016 Oct 4. Acc Chem Res. 2016. PMID: 27700084
The effect of amino acid additives (N-Boc-glycine) was further investigated during the indium-mediated allylation of isatins with allyl bromide to yield homoallylic alcohols in excellent yields in a short time with a wide range of functional group tolerance. Critica …
The effect of amino acid additives (N-Boc-glycine) was further investigated during the indium-mediated allylation of isatins with allyl …
Oligonucleotide nanoassemblies with allyl bromide scaffold-based small molecules.
Abbas SJ, Yesmin S, Xia F, Ali SI, Xiao Z, Tan W. Abbas SJ, et al. Discov Nano. 2023 Jun 3;18(1):81. doi: 10.1186/s11671-023-03846-0. Discov Nano. 2023. PMID: 37382753 Free PMC article.
However, the interaction of negatively charged oligonucleotides with halogenated small molecules represents a scientific challenge. Here, we introduced a distinct allyl bromide halogenated scaffold, which exhibits specific interaction with adenine nucleic bases of t …
However, the interaction of negatively charged oligonucleotides with halogenated small molecules represents a scientific challenge. Here, we …
Synthesis and crystal structure of allyl 7-(di-ethyl-amino)-2-oxo-2H-chromene-3-carboxyl-ate.
Nowatschin V, Näther C, Lüning U. Nowatschin V, et al. Acta Crystallogr E Crystallogr Commun. 2021 Mar 2;77(Pt 4):331-334. doi: 10.1107/S2056989021002218. eCollection 2021 Apr 1. Acta Crystallogr E Crystallogr Commun. 2021. PMID: 33936752 Free PMC article.
The title compound, C(17)H(19)NO(4), was synthesized by the reaction of 7-(di-ethyl-amino)-2-oxo-2H-chromene-3-carb-oxy-lic acid with allyl bromide and purified by flash column chromatography on silica gel. ...
The title compound, C(17)H(19)NO(4), was synthesized by the reaction of 7-(di-ethyl-amino)-2-oxo-2H-chromene-3-carb-oxy-lic acid with all …
A base-mediated synthesis of N-hydroxy- and N-alkoxyindoles from 2-nitrostyrenes.
McClay BT, Lambson KE, Banini SR, Akhmedov TN, Söderberg BCG. McClay BT, et al. Tetrahedron. 2023 Sep 7;144:133578. doi: 10.1016/j.tet.2023.133578. Epub 2023 Aug 6. Tetrahedron. 2023. PMID: 37680993
Sequential treatment of alkyl 2-(2-nitroaryl)-2-butenoates with potassium tert-butoxide and an electrophile, such as methyl iodide, benzyl bromide and allyl bromide, afforded N-alkoxyindoles. In related reactions, using sodium tert-pentoxide as the base with or with …
Sequential treatment of alkyl 2-(2-nitroaryl)-2-butenoates with potassium tert-butoxide and an electrophile, such as methyl iodide, benzyl b …
Redox-Active Ligand-Assisted Two-Electron Oxidative Addition to Gallium(II).
Fedushkin IL, Dodonov VA, Skatova AA, Sokolov VG, Piskunov AV, Fukin GK. Fedushkin IL, et al. Chemistry. 2018 Feb 6;24(8):1877-1889. doi: 10.1002/chem.201704128. Epub 2018 Jan 17. Chemistry. 2018. PMID: 29125198
Treatment of complex 4 with pyridine induced an intramolecular redox process, which resulted in the diamagnetic complex (dpp-bian)Ga(Py)Cl (5). In reaction with allyl bromide, complex 2 gave metal- and ligand-centered addition products (dpp-bian)Ga(eta(1) -All)Br (6 …
Treatment of complex 4 with pyridine induced an intramolecular redox process, which resulted in the diamagnetic complex (dpp-bian)Ga(Py)Cl ( …
Total synthesis of alotaketal A.
Xuan M, Paterson I, Dalby SM. Xuan M, et al. Org Lett. 2012 Nov 2;14(21):5492-5. doi: 10.1021/ol302570k. Epub 2012 Oct 24. Org Lett. 2012. PMID: 23094646
A convergent approach to the unusual alotane sesterterpenoid skeleton was employed, exploiting a remarkable LiDBB-mediated coupling of an (R)-carvone-derived delta-lactone with an allyl bromide side chain, followed by spiroacetalization....
A convergent approach to the unusual alotane sesterterpenoid skeleton was employed, exploiting a remarkable LiDBB-mediated coupling of an (R …
A Thioether-Catalyzed Cross-Coupling Reaction of Allyl Halides and Arylboronic Acids.
Xu J, He Z, Zhang J, Chen J, Huang Y. Xu J, et al. Angew Chem Int Ed Engl. 2022 Oct 24;61(43):e202211408. doi: 10.1002/anie.202211408. Epub 2022 Sep 14. Angew Chem Int Ed Engl. 2022. PMID: 36042000
Herein, we report our recent discovery of a designer thioether as a highly active organocatalyst for reactions between an allyl bromide and an arylboronic acid. The cross-coupling event occurred readily under mild condition in the presence of a weak inorganic base. …
Herein, we report our recent discovery of a designer thioether as a highly active organocatalyst for reactions between an allyl br …
Stereospecific 7α-alkylation of 20-hydroxyecdysone in a lithium-ammonia solution.
Galyautdinov IV, Khairullina ZR, Zaripova ER, Sametov VP, Mescheryakova ES, Muslimov ZS, Mozgovoi OS, Khalilov LM, Odinokov VN. Galyautdinov IV, et al. Steroids. 2015 Jun;98:122-5. doi: 10.1016/j.steroids.2015.03.002. Epub 2015 Mar 14. Steroids. 2015. PMID: 25777947
The reaction of 20-hydroxyecdysone with methyl or ethyl iodide or allyl bromide in a lithium-ammonia solution results in stereospecific 7alpha-alkylation to give 7alpha-methyl-, 7alpha-ethyl-, and 7alpha-allyl-14-deoxy-delta(8(14))-20-hydroxyecdysones, respectively. …
The reaction of 20-hydroxyecdysone with methyl or ethyl iodide or allyl bromide in a lithium-ammonia solution results in stere …
Nematicidal activity of allyl bromide and dibromo(nitro)methane under laboratory conditions.
Oka Y, Shuker S, Tkachi N. Oka Y, et al. Pest Manag Sci. 2016 Jan;72(1):57-66. doi: 10.1002/ps.4001. Epub 2015 Apr 8. Pest Manag Sci. 2016. PMID: 25754847
Allyl bromide also showed higher nematicidal activity than dibromo(nitro)methane against M. javanica and P. penetrans in soil. ...No P. penetrans were recovered from soil treated with 80 mg allyl bromide L(-1) soil or 320 mg dibromo(nitro)methane L(-1) …
Allyl bromide also showed higher nematicidal activity than dibromo(nitro)methane against M. javanica and P. penetrans in soil. …
216 results