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Hydride-Containing Eight-Electron Pt/Ag Superatoms: Structure, Bonding, and Multi-NMR Studies.
Chiu TH, Liao JH, Gam F, Wu YY, Wang X, Kahlal S, Saillard JY, Liu CW. Chiu TH, et al. J Am Chem Soc. 2022 Jun 15;144(23):10599-10607. doi: 10.1021/jacs.2c03715. Epub 2022 Jun 2. J Am Chem Soc. 2022. PMID: 35654753 Free article.
Whereas the multi-NMR spectra of 2 in solution at 173 K reveal that the structure of C(3) symmetry is the predominant one, (1)H and (195)Pt NMR spectra of 1 at the same temperature disclose the presence of isomers of both C(1) and C(3) symmetry. ...They also show that the …
Whereas the multi-NMR spectra of 2 in solution at 173 K reveal that the structure of C(3) symmetry is the predominant one, (1)H and ( …
Zipper-like Watson-Crick base-pairs.
Chou SH, Chin KH. Chou SH, et al. J Mol Biol. 2001 Sep 28;312(4):753-68. doi: 10.1006/jmbi.2001.4962. J Mol Biol. 2001. PMID: 11575930
Such oligomers reveal excellent resolution in NMR spectra and exhibit many unusual nuclear Overhauser effects (NOEs) that allow for good characterization of an unusual zipper-like conformation with zipper-like Watson-Crick base-pairs; the potential canonical X.Y H-bonding …
Such oligomers reveal excellent resolution in NMR spectra and exhibit many unusual nuclear Overhauser effects (NOEs) that allow for good cha …
Breed-specific differences in the immune response to lipopolysaccharide in ewes.
Hadfield JM, Bowdridge EC, Holásková I, Elsasser TH, Dailey RA. Hadfield JM, et al. J Anim Sci. 2018 Sep 29;96(10):4220-4228. doi: 10.1093/jas/sky288. J Anim Sci. 2018. PMID: 30107562 Free PMC article.
Blood was collected via jugular venipuncture intermittently for 24 h to determine WBC counts. Rectal temperatures and observations of behavioral/physical appearances were recorded hourly. ...Overall, Dorset ewes had greater expression of TLR4 (P = 0.003), IL-10 (P = 0.045) …
Blood was collected via jugular venipuncture intermittently for 24 h to determine WBC counts. Rectal temperatures and observations of …
Folate receptor targeted alpha-therapy using terbium-149.
Müller C, Reber J, Haller S, Dorrer H, Köster U, Johnston K, Zhernosekov K, Türler A, Schibli R. Müller C, et al. Pharmaceuticals (Basel). 2014 Mar 13;7(3):353-65. doi: 10.3390/ph7030353. Pharmaceuticals (Basel). 2014. PMID: 24633429 Free PMC article.
It decays by emission of short-range alpha-particles (Ealpha = 3.967 MeV) with a half-life of 4.12 h. The goal of this study was to investigate the anticancer efficacy of a 149Tb-labeled DOTA-folate conjugate (cm09) using folate receptor (FR)-positive cancer cells in vitro …
It decays by emission of short-range alpha-particles (Ealpha = 3.967 MeV) with a half-life of 4.12 h. The goal of this study was to i …
Novel functional M1 selective muscarinic agonists. Synthesis and structure-activity relationships of 3-(1,2,5-thiadiazolyl)-1,2,5,6-tetrahydro-1-methylpyridines.
Sauerberg P, Olesen PH, Nielsen S, Treppendahl S, Sheardown MJ, Honoré T, Mitch CH, Ward JS, Pike AJ, Bymaster FP, et al. Sauerberg P, et al. J Med Chem. 1992 Jun 12;35(12):2274-83. doi: 10.1021/jm00090a019. J Med Chem. 1992. PMID: 1613751
Depicting chain length against Oxo-M binding and against Pz binding the unbranched C1-8 alkoxy-TZTP (5a-h) derivatives produced U-shaped curves with butoxy- (5d) and (pentyloxy)-TZTP (5e) as the optimum chain length, respectively. ...In both the atria and in the ile …
Depicting chain length against Oxo-M binding and against Pz binding the unbranched C1-8 alkoxy-TZTP (5a-h) derivatives produced U-sha …
Syntheses, reactivity, and crystal structures of molybdenum complexes with pyridine-2-thionate (pyS)-containing ligands: crystal structures of [Mo(eta(3)-C(3)H(5))(CO)(2)](2)(mu-eta(1),eta(2)-pyS)(2), exo-[Mo(eta(3)-C(3)H(5))(CO)(eta(2)-pyS)(eta(2)-dppe)], [Mo(CO)(3)(eta(1)-SC(5)H(4)NH)(eta(2)-dppm)], and [Mo(CO)(eta(2)-pyS)(2)(eta(2)-dppm)].
Yih KH, Lee GH, Wang Y. Yih KH, et al. Inorg Chem. 2003 Feb 24;42(4):1092-100. doi: 10.1021/ic020579x. Inorg Chem. 2003. PMID: 12588143
Four conformational isomers, endo,exo-complexes [Mo(eta(3)-C(3)H(5))(CO)(eta(2)-pyS)(eta(2)-diphos)] (diphos = dppm, 4a-4d; dppe, 5a-5d), are accessible by the reactions of 1 with dppm and dppe in refluxing acetonitrile. Homonuclear shift-correlated 2-D (31)P((1) …
Four conformational isomers, endo,exo-complexes [Mo(eta(3)-C(3)H(5))(CO)(eta(2)-pyS)(eta(2)-diphos)] (diphos = dppm, 4a-4d; dppe, 5a- …
Synthesis and Crystallographic Characterization of a Reduced Bimetallic Yttrium ansa-Metallocene Hydride Complex, [K(crypt)][(mu-Cp(An))Y(mu-H)](2) (Cp(An) = Me(2)Si[C(5)H(3)(SiMe(3))-3](2)), with a 3.4 A Yttrium-Yttrium Distance.
Wedal JC, Anderson-Sanchez LM, Dumas MT, Gould CA, Beltrán-Leiva MJ, Celis-Barros C, Páez-Hernández D, Ziller JW, Long JR, Evans WJ. Wedal JC, et al. J Am Chem Soc. 2023 May 17;145(19):10730-10742. doi: 10.1021/jacs.3c01405. Epub 2023 May 3. J Am Chem Soc. 2023. PMID: 37133919
The reduction of a bimetallic yttrium ansa-metallocene hydride was examined to explore the possible formation of Y-Y bonds with 4d(1) Y(II) ions. The precursor [Cp(An)Y(mu-H)(THF)](2) (Cp(An) = Me(2)Si[C(5)H(3)(SiMe(3))-3](2)) was synthesized by hydrogenolysis of th …
The reduction of a bimetallic yttrium ansa-metallocene hydride was examined to explore the possible formation of Y-Y bonds with 4d(1) Y(II) …
Enhanced Catalytic Ozonation for Eliminating CH3SH via Graphene-Supported Positively Charged Atomic Pt Undergoing Pt2+/Pt4+ Redox Cycle.
Huang Y, Ma D, Liu W, Xia D, Hu L, Yang J, Liao P, He C. Huang Y, et al. Environ Sci Technol. 2021 Dec 21;55(24):16723-16734. doi: 10.1021/acs.est.1c06938. Epub 2021 Dec 9. Environ Sci Technol. 2021. PMID: 34882404
A CH(3)SH removal efficiency of 91.5% can be obtained during catalytic ozonation using optimum 0.5AD-Pt-G within 12 h under a gas hourly space velocity of 60,000 mL h(-1) g(-1), whereas that of pure graphene is 40.4%. ...Moreover, the results of XPS and DFT calculat …
A CH(3)SH removal efficiency of 91.5% can be obtained during catalytic ozonation using optimum 0.5AD-Pt-G within 12 h under a gas hou …
Molecular Modeling Studies of Novel Fluoroquinolone Molecules.
Allaka TR, Katari NK, Veeramreddy V, Anireddy JS. Allaka TR, et al. Curr Drug Discov Technol. 2018;15(2):109-122. doi: 10.2174/1570163814666170829142044. Curr Drug Discov Technol. 2018. PMID: 28875852
The compounds in general exhibited good binding interactions like H-bonding interaction and pi-pi interactions which stabilize the protein-ligand complexes and responsible for good fitness scores in both the protocols. ...From the docking study, we have explored the probab …
The compounds in general exhibited good binding interactions like H-bonding interaction and pi-pi interactions which stabilize the pr …
First detection of doubly deuterated methyl acetylene (CHD2CCH and CH2DCCD)★.
Agúndez M, Roueff E, Cabezas C, Cernicharo J, Marcelino N. Agúndez M, et al. Astron Astrophys. 2021 Jun 1;649:A171. doi: 10.1051/0004-6361/202140843. eCollection 2021 May. Astron Astrophys. 2021. PMID: 34334795 Free PMC article.
The abundances of the different deuterated isotopologues with respect to CH(3)CCH are reasonably accounted for by a gas-phase chemical model in which deuteration occurs from the precursor ions C(3)H(6)D(+) and C(3)H(5)D(+), when the ortho-to-para ratio of molecular …
The abundances of the different deuterated isotopologues with respect to CH(3)CCH are reasonably accounted for by a gas-phase chemical model …
57 results